oa South African Journal of Chemistry - Microwave-assisted synthesis of some 1H-1,2,4-triazol-3-one derivatives : research article
|Article Title||Microwave-assisted synthesis of some 1H-1,2,4-triazol-3-one derivatives : research article|
|© Publisher:||South African Chemical Institute (SACI)|
|Journal||South African Journal of Chemistry|
|Affiliations||1 Recep Tayyip Erdogan University, Turkey, 2 Recep Tayyip Erdogan University, Turkey, 3 Recep Tayyip Erdogan University, Turkey, 4 Recep Tayyip Erdogan University, Turkey and 5 Karadeniz Technical University, Turkey|
|Publication Date||Jan 2013|
|Pages||72 - 76|
|Keyword(s)||Hydrazine hydrate, Microwave irradiation, Oxadiazole and Triazole|
4-Amino-5-(methyl/ethyl)-2,4-dihydro-3H-1,2,4-triazol-3-one were synthesized from the reaction of (methyl/ethyl)-ester ethoxycarbonyl hydrazone with hydrazine hydrate and then, converted to corresponding Schiff bases using 9H-fluorene-3-carbaldehyde. Ester, hydrazide and oxadiazole derivatives were synthesized starting from Schiff bases in three steps. All reactions occurred under conventional conditions and microwave irradiation. The obtained results were compared.
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